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Blind QC Quarter II 2018 Report43247/30/2018 3:13:16 PMAlthough not written in the section’s SOP, it is the duty of the section supervisors to The Toxicology section began doing in-house drug confirmation in June 2018 and 5https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Verification_ALC_HS-2_2018-07-1342347/12/2018 6:25:13 PMPurpose To show the instrument is fit for use after completion of annual  preventative by Headspace GC-FID section of the Toxicology Section Analytical Manual Standard Operating https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf

HFSC Quality Manual eff 07.05.201841717/5/2018 7:13:35 AMHouston Forensic Science Center Quality Manual Quality DivisionHouston Forensic Science Center HFSC Quality Manual Quality Division HFSC Quality Manual Document ID: 1105 Issued By https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
SOQ_TS41557/3/2018 8:46:49 AMUncertainty in Forensic Chemistry‐February 2010; SOP  writing for ISO 17025‐ February 2010; Uncertainty in Forensic Chemistry and Toxicology II‐ March  2009; Drug Facts: DFSA https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
2018-04441607/3/2018 1:37:54 PMClient Services/Case Management (CS/CM) SOP clause 3.2. and Toxicology Analytical Manual v 3.1 clause 3.8. However, it was 7https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
SOQ_DM43647/17/2018 2:54:19 PMother duties as assigned by the toxicology managers and the Director of Toxicology and Chemistry -Supervising the workflow in the GC/MS section of the toxicology laboratory https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Verification_EIA_Tecan-2_Eff 2018-06-2741786/27/2018 12:53:24 PMPurpose Analytes Units of Measure Analyst Performing Validation Study Responsible Supervisor Start Date Completion Date Primary Matrix Blood & Urine Calibrator Concentration https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
SOQ_CLR41026/25/2018 1:22:42 PMCenter  JOB TITLE:  Forensic Analyst ‐ Toxicology    Indicate all disciplines in which you Forensic Toxicology Testimony: “How to Effectively Communicate Our Science to the Courts 12https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
2018-04241036/25/2018 9:19:58 AMThe analyst notified the Toxicology manager, Toxicology supervisor, CS/CM manager and CS SOPs are appropriate for the work being done and will not be revised due to this incident https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Training Guide for General Analysis issued 2018-06-1139676/11/2018 11:19:34 AMSeized Drugs Training Guide for General Analysis Comparative and Analytical Division Seized Drugs Training Guide for General Analysis Comparative & Analytical Division https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Verification_THC_Blood_Eff 2018-06-06_39576/6/2018 3:30:28 PMTo ensure the newly prepared solutions meet the acceptance criteria and are valid for use in casework Std err in slope, S b There was no outlier found but there Deviations from SOP https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Training Manual_v3.2_Eff 2018-05-09 to Present34865/8/2018 7:52:18 AM1.2.2. Scope: The training covers the SOPs implemented within the HFSC Toxicology Section of analytical assays currently in service within the Toxicology Section are also included 31https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Verification_ALC_HS-2_Eff 2018-05-0834885/8/2018 10:30:09 AMby Headspace GC-FID section of the Toxicology Section Analytical Manual Standard Operating for semi-quantitative confirmation only and therefore meets acceptance criteria per SOP https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Verification_BNZ_Urine_Eff 2018-05-0235935/2/2018 10:15:47 AMPurpose To ensure the newly prepared oxazepam-glucuronide control meets the acceptance Date April 4, 2018 Deviations from SOP: Other Observations: Recommended Maximum Run Length https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Validation_BNZ_Urine_Eff 2018-04-2736144/26/2018 3:41:19 PMis documented in Journal of Analytical Toxicology, 2016 Oct; 40(8):663-668. Epub 2016 any deviation from that described in the SOP as determined by the Supervisor 3 N=Negative https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Verification_BNZ_Blood_Eff 2018-04-27_Updated 2018-05-2436335/24/2018 4:01:12 PMForensic Science Center, ou=Toxicology, email=mhenry@houstonforensicscience.org, c=US Date dates/reasons): Date Deviations from SOP: Recommended Maximum Run Length (# unknown https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Validation_EIA_Urine_Tecan_2018-04-2334223/14/2018 11:38:06 AMPurpose To demonstrate the validated method from Tecan-2 is suitable for casework on Tecan ELISA) section 12.9 of the Toxicology Section Analytical Manual - Standard Operating https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
2018-01734194/19/2018 1:25:09 PMplaced the evidence back into Toxicology Refrigerator-3 in order to accession the next day The accessioner reviewed the SOP and completed a quiz through Qualtrax on 03/13/2018 as 7https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Verification_BSD_Blood_Eff 2018-04-1835914/18/2018 9:28:14 AMPurpose To ensure the newly prepared calibrator and control solutions meet the acceptance reasons): Date N/A Deviations from SOP: Other Observations: Recommended Maximum Run Length 3https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Internal Audit_2018-04-1734164/16/2018 3:52:17 PMSection 9.3.2.1. of the toxicology SOP states that “All maintenance and repairs should be Re-classify evidence photographs in the Toxicology SOP section 4.5.3 from administrative 17https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Verification_BNZ_Blood_Eff 2018-04-0235944/2/2018 4:26:02 PMPurpose To show the method is fit for purpose after reprocessing the  data the acceptance criteria of the Toxicology Analytical Manual 3.1. The updated method (ALP https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Validation_THC_Blood_Eff 2018-03-2836053/20/2018 9:21:51 AMvalue METHOD VALIDATION PROTOCOL AND RESULTS SOP REFERENCE v3.1 4 * Alternate criteria is any deviation from that described in the SOP as determined by the Supervisor Not performed 3https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Validation_COC_Blood_Eff 2018-03-1436113/7/2018 1:29:47 PMfrom labeled IS. METHOD VALIDATION PROTOCOL AND RESULTS SOP REFERENCE v3.1 4 Not performed is any deviation from that described in the SOP as determined by the Supervisor If method https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Validation_AMP_Blood_Eff 2018-03-1436213/7/2018 9:15:57 AMYDOXH METHOD VALIDATION PROTOCOL AND RESULTS SOP REFERENCE v3.1 * Alternate criteria is any deviation from that described in the SOP as determined by the Supervisor %LDV 3https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Verification_ALC_HS-3_Eff 2018-03-1233113/12/2018 12:26:56 PMPurpose To show the instrument is fit for use after trimming the inlet column by Headspace GC-FID section of the Toxicology Section Analytical Manual Standard Operating https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Training Manual_v3.1_Eff 2018-02-28 to 2018-05-0834875/8/2018 9:01:42 AMby Section Manager -DL 2018-05-08 Toxicology Training Manual_v3.1 Comparative & Analytical The Toxicology Training Program should familiarize the trainee with the relevant policies https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
UM_ALC_Eff 2018-02-2732522/6/2018 1:45:01 PMAnalyte Ethanol, Methanol, Isopropanol, Acetone Units of Measure g/100 mL Analyst Duplicate analysis Type B: Duplicate Agreement SOP allowance of 5% at specification limit https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Analytical Manual_v3.1_Eff 2018-02-21 to Present32482/20/2018 11:34:30 AM1. Introduction 1.1. This Toxicology Standard Operating Procedures manual (“manual” or “SOP manual”) is intended to consolidate the 6https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Validation_PCP_Blood_Eff 2018-02-1636072/14/2018 9:01:04 AMMETHOD VALIDATION PROTOCOL AND RESULTS SOP REFERENCE v3.1 4 * Alternate criteria is any deviation from that described in the SOP as determined by the Supervisor 8 Bias: ≤ 20 https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
2018 Biology_SOP issued 02-14-2018_39464/27/2018 5:01:33 PMBiology SOP Document ID: 3664 Issued By: Section Technical Leader Issue Date 1.4. This SOP is only one part of the policies and procedures that govern all work https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Verification_THC_Blood_Eff 2018-02-1335762/12/2018 2:34:32 PMCannabinoids (Δ-9-tetrahydrocannabinol (THC), 11-hydroxy-THC (11-OH-THC), 11-nor-9-carboxy-THC 9/13/2017 9/19/2017 Deviations from SOP: Other Observations: Recommended Maximum Run 3https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Verification_OPI_Blood_Eff 2018-02-1235882/12/2018 2:33:22 PMStd err in slope, S b https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Verification_BNZ_Blood_Eff 2018-02-1235952/12/2018 2:35:42 PMStd err in slope, S b dates/reasons): Date Deviations from SOP: Other Observations: Recommended Maximum Run https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Verification_COC_Blood_Eff 2018-02-0935472/9/2018 4:04:17 PMStd err in slope, S b https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Verification_PCP_Blood Eff 2018-02-0935852/9/2018 4:05:15 PMThey both produced acceptable results, so the SOP was changed to fortify calibrators and used to verify the SOP change; PCP_20170914B_MRL, PCP_20170920B_LL, and PCP_20170926B_TS https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Validation_EIA_Tecan-2_Urine_Eff 2018-02-0831142/1/2018 11:52:30 AMPurpose To demonstrate that the new instrument, increasing sample  dilution with PBS from 1:10 to 1:20, and increasing the Positive  Control concentration for barbiturates https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Validation_EIA_Tecan-2_Blood_Eff 2018-02-0831152/1/2018 10:42:16 AMPurpose To demonstrate that the new instrument is valid for use in  casework Analytes Amphetamines, Barbiturates, Benzodiazepines, Cocaine and  metabolites, Cannabinoids 433https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
UM_BNZ_Blood_Eff 2018-01-2636261/10/2018 3:31:41 PMAnalyte Benzodiazepines (Nordiazepam, Oxazepam, Lorazepam, Temazepam, α-Hydroxyalprazolam of NIST traceable flasks as described in SOP version 3.1. Dilution of CRM to working https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Verification_AMP_Blood_Eff 2018-01-2236031/22/2018 1:10:36 PMStd err in slope, S b Bias: ≤ ±20%; Within-Run Imprecision: CV ≤ ±20%; Between-Run Imprecision: CV ≤ ±20 Number in red is an outlier The calculated concentration is within 20% of the https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Validation_OPI_Blood_Eff 2018-01-0936091/4/2018 9:25:28 AM100% of samples ≤ 20% of target value SOP REFERENCE v3.1 Red values indicate ion ratios deviation from that described in the SOP as determined by the Supervisor METHOD VALIDATION https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Validation_BNZ_Blood_Eff 2018-01-0936151/5/2018 4:10:54 PMM Matrix: Blood Instrument: GCMS-5 SOP CRITERIA ALTERNATE CRITERIA* RESULTS VALIDATION : IS Interference: Comments: Acceptance Criteria: No matrix interference was identified. There https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
UM_AMP_Blood_Eff 2018-01-0936271/5/2018 3:32:07 PMAnalyte Amphetamines (Amphetamine, Methamphetamine, 3,4-Methylenedioxymethamphetamine (MDMA), 3 of NIST traceable flasks as described in SOP version 3.1. Dilution of CRM to working https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Validation_THC_Urine_Eff 2017-12-20360412/15/2017 2:49:56 PMM Matrix: Urine Instrument: GCMS-4 SOP CRITERIA ALTERNATE CRITERIA* RESULTS VALIDATION cannabis". METHOD VALIDATION PROTOCOL AND RESULTS SOP REFERENCE: v3.1 1 Precision around https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Validation_OPI_Urine_Eff 2017-12-20360812/15/2017 2:32:05 PMOpioids (Hydrocodone, Hydromorphone, Oxycodone, Oxymorphone, Codeine SOP REFERENCE v3.1 criteria is any deviation from that described in the SOP as determined by the Supervisor https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Validation_AMP_Urine_Eff 2017-12-20362012/20/2017 9:00:20 AMAnalyte Amphetamines (Amphetamine, Methamphetamine, 3,4-Methylenedioxymethamphetamine (MDMA), 3,4-Methylene-N-dioxyethylamphetamine (MDEA)) Units of SOP CRITERIA SOP REFERENCE v3.1 https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
UM_THC_Blood_Eff 2017-12-20362212/18/2017 3:00:23 PMAnalyte THC (delta-9-tetrahydrocannabinol (THC), 11-hydroxy-THC (11-OH-THC of NIST traceable flasks as described in SOP version 3.1. Dilution of working solution A https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Validation_COC_Urine_Eff 2017-12-18361011/29/2017 3:53:09 PMStability Samples must test positive SOP REFERENCE v3.1 * Alternate criteria is any deviation from that described in the SOP as determined by the Supervisor: n/a 1 https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
UM_COC_Blood_Eff 2017-12-18362511/27/2017 4:26:29 PMAnalyte Cocaine (Benzoylecgonine (BE), Cocaine (COC) Cocaethylene (CE)) Units of Measure ng/mL of NIST traceable flasks as described in SOP version 3.1. Dilution of CRM to working https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
HFSC Quality Manual eff 12.15.1733253/27/2018 7:48:13 AM Houston Forensic Science Center HFSC Quality Manual Quality Division HFSC Quality Manual Document ID: 1105 Issued By: Quality Director Issue Date: 12/15/2017December 15, 2017 149https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf
Validation_PCP_Urine_Eff 2017-12-15360612/13/2017 9:53:30 AMPCP.M Matrix: Urine Instrument: GCMS-4 SOP REFERENCE v3.1 SOP CRITERIA ALTERNATE CRITERIA* RESULTS VALIDATION COMMENTS 3https://records.hfscdiscovery.org/Published/Forms/AllItems.aspxpdfFalsepdf